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xtalab synergy-s dualflex diffractometer equipped with a hypix-6000he hpc area detector  (Rigaku Corporation)


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    Rigaku Corporation xtalab synergy-s dualflex diffractometer equipped with a hypix-6000he hpc area detector
    Xtalab Synergy S Dualflex Diffractometer Equipped With A Hypix 6000he Hpc Area Detector, supplied by Rigaku Corporation, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/product/xtalab+synergy+diffractometer+with+a+dualflex+hypix+detector/hypix+6000he+detector/10__1021_slash_acselectrochem__4c00186-89-27-19
    Average 90 stars, based on 1 article reviews
    xtalab synergy-s dualflex diffractometer equipped with a hypix-6000he hpc area detector - by Bioz Stars, 2026-10
    90/100 stars

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    Article Title: High-resolution structural study on pyridin-3-yl ebselen and its <i>N</i>-methylated tosylate and iodide derivatives
    Article Snippet: C79, 43-51 C10—C11—C12—C8 −0.5 (5) C19—C14—S1—O4 158.2 (2) N1—C8—C12—C11 −178.3 (3) C15—C14—S1—O4 −24.3 (3) C9—C8—C12—C11 0.4 (4) C19—C14—S1—O3 36.0 (3) C19—C14—C15—C16 −0.8 (4) C15—C14—S1—O3 −146.4 (2) S1—C14—C15—C16 −178.3 (2) C19—C14—S1—O2 −81.8 (2) C14—C15—C16—C17 0.7 (4) C15—C14—S1—O2 95.7 (2) C15—C16—C17—C18 −0.1 (4) Hydrogen-bond geometry (Å, o) D—H···A D—H H···A D···A D—H···A C6—H6···O2 0.93 2.28 2.925 (4) 126 C9—H9···O1 0.93 2.09 2.734 (4) 125 C10—H10···O3i 0.93 2.37 3.216 (4) 152 C11—H11···O7i 0.93 2.46 3.338 (4) 158 C12—H12···Se1 0.93 2.61 3.085 (3) 112 C13—H13B···O3i 0.96 2.57 3.442 (4) 152 C13—H13C···O4ii 0.96 2.54 3.490 (4) 170 C15—H15···O1ii 0.93 2.63 3.379 (4) 138 O5—H5A···O3 0.82 (1) 1.99 (1) 2.786 (3) 166 (4) O5—H5A···S1 0.82 (1) 3.01 (2) 3.698 (2) 144 (3) O5—H5B···O7 0.82 (1) 1.99 (4) 2.758 (3) 155 (8) O6—H6A···O4 0.82 (1) 2.27 (2) 3.045 (3) 159 (5) O6—H6B···O5 0.82 (1) 1.99 (2) 2.782 (4) 162 (7) O7—H7A···O6iii 0.82 (1) 1.97 (1) 2.783 (4) 176 (5) O7—H7B···O5iv 0.82 (1) 1.97 (1) 2.786 (4) 172 (6) Symmetry codes: (i) x, y−1, z; (ii) −x+2, −y+1, −z+1; (iii) −x+2, −y+2, −z+2; (iv) −x+1, −y+2, −z+2. (2-multipole) Crystal data C12H8N2OSe Mr = 275.16 Monoclinic, P21/n a = 6.1074 (1) Å b = 14.2227 (3) Å c = 12.0621 (2) Å β = 103.588 (2)° V = 1018.43 (3) Å3 Z = 4 F(000) = 544.0 Dx = 1.795 Mg m−3 Mo Kα radiation, λ = 0.71073 Å Cell parameters from 30292 reflections θ = 3.3–56.9° μ = 3.66 mm−1 T = 100 K Plate, colourless 0.48 × 0.15 × 0.05 mm Data collection Rigaku XtaLAB Synergy diffractometer with a Dualflex HyPix detector Detector resolution: 10.0000 pixels mm-1 ω scans Absorption correction: gaussian (CrysAlis PRO; Rigaku OD, 2020) Tmin = 0.147, Tmax = 1.000 97589 measured reflections 7174 independent reflections 6298 reflections with I ≥ 2u(I) Rint = 0.044 θmax = 42.5°, θmin = 2.3° h = −11→11 k = 0→27 l = 0→22 supporting information sup-13Acta Cryst. (2023).

    Article Title: Structural phase transition in a charge-transfer compound: tropylium hexafluoridoantimonate(V)–1,4-dimethylnaphthalene (1/1)
    Article Snippet: Molecular motion in crystals has attracted much attention for the development of stimuli-responsive materials.. The most studied are molecules with few atoms or highly symmetrical molecules.. To develop molecules with new motion characteristics, we synthesized a charge-transfer compound, namely, tropylium hexafluoridoantimonate(V)–1,4-dimethylnaphthalene (1/1), (C7H7)[SbF6] C12H12, and studied its structural phase transition.

    Article Title: High-resolution structural study on pyridin-3-yl ebselen and its <i>N</i>-methylated tosylate and iodide derivatives
    Article Snippet: 1-Methyl-3-(3-oxo-2,3-dihydro-1,2-benzoselenazol-2-yl)pyridin-1-ium iodide (2-MeIodide) Crystal data C13H11N2OSe+·I− Mr = 417.10 Triclinic, P1 a = 7.0926 (1) Å b = 8.1329 (1) Å c = 11.8376 (1) Å α = 84.618 (1)° β = 82.243 (1)° γ = 77.756 (1)° V = 659.70 (1) Å3 Z = 2 F(000) = 396 Dx = 2.100 Mg m−3 Mo Kα radiation, λ = 0.71073 Å Cell parameters from 41098 reflections θ = 3.0–51.1° μ = 5.18 mm−1 T = 100 K Needle, pale yellow 0.46 × 0.06 × 0.06 mm Data collection Rigaku XtaLAB Synergy diffractometer with a Dualflex HyPix detector Radiation source: micro-focus sealed X-ray tube, PhotonJet (Mo) X-ray Source Mirror monochromator ω scans Absorption correction: gaussian (CrysAlis PRO; Rigaku OD, 2020) Tmin = 0.351, Tmax = 1.000 90106 measured reflections 14487 independent reflections 12038 reflections with I > 2σ(I) Rint = 0.055 θmax = 51.3°, θmin = 2.6° h = −15→14 k = −17→17 l = −25→25 Refinement Refinement on F2 Least-squares matrix: full R[F2 > 2σ(F2)] = 0.025 wR(F2) = 0.058 S = 1.03 14487 reflections 164 parameters 0 restraints Hydrogen site location: inferred from neighbouring sites H-atom parameters constrained supporting information sup-5Acta Cryst. (2023).

    Article Title: High-resolution structural study on pyridin-3-yl ebselen and its <i>N</i>-methylated tosylate and iodide derivatives
    Article Snippet: C79, 43-51 Se1—C1—C2—C7 1.17 (9) C9—C8—C12—C11 −0.79 (12) C1—C2—C3—C4 −0.60 (12) O1—C7—N1—C8 −2.54 (13) C7—C2—C3—C4 −179.28 (8) C2—C7—N1—C8 178.26 (7) C2—C3—C4—C5 −0.34 (13) O1—C7—N1—Se1 −179.84 (7) C3—C4—C5—C6 0.70 (14) C2—C7—N1—Se1 0.97 (8) C4—C5—C6—C1 −0.11 (13) C9—C8—N1—C7 −1.69 (12) C2—C1—C6—C5 −0.83 (12) C12—C8—N1—C7 178.33 (8) Se1—C1—C6—C5 177.74 (6) C9—C8—N1—Se1 175.46 (6) C1—C2—C7—O1 179.39 (8) C12—C8—N1—Se1 −4.52 (10) C3—C2—C7—O1 −1.90 (13) C11—C10—N2—C9 −1.72 (13) C1—C2—C7—N1 −1.40 (10) C11—C10—N2—C13 178.35 (8) C3—C2—C7—N1 177.32 (7) C8—C9—N2—C10 1.26 (12) N1—C8—C9—N2 −179.95 (7) C8—C9—N2—C13 −178.82 (8) C12—C8—C9—N2 0.03 (12) 1-Methyl-3-(3-oxo-2,3-dihydro-1,2-benzoselenazol-2-yl)pyridin-1-ium toluenesulfonate trihydrate (2- Metosylate) Crystal data C13H11N2OSe+·C7H7O3S−·3H2O Mr = 515.43 Triclinic, P1 a = 6.9412 (3) Å b = 12.1279 (4) Å c = 13.5994 (3) Å α = 70.426 (3)° β = 83.774 (3)° γ = 83.585 (3)° V = 1068.83 (7) Å3 Z = 2 F(000) = 528 Dx = 1.602 Mg m−3 Cu Kα radiation, λ = 1.54184 Å Cell parameters from 5181 reflections θ = 3.5–75.2° μ = 3.70 mm−1 T = 100 K Rod, colourless 0.21 × 0.03 × 0.03 mm Data collection Rigaku XtaLAB Synergy diffractometer with a Dualflex HyPix detector Radiation source: micro-focus sealed X-ray tube, PhotonJet (Cu) X-ray Source Mirror monochromator ω scans Absorption correction: multi-scan (CrysAlis PRO; Rigaku OD, 2020) Tmin = 0.668, Tmax = 1.000 15253 measured reflections 4435 independent reflections 3777 reflections with I > 2σ(I) Rint = 0.064 θmax = 77.1°, θmin = 3.5° h = −8→8 k = −15→14 l = −17→12 Refinement Refinement on F2 Least-squares matrix: full R[F2 > 2σ(F2)] = 0.041 wR(F2) = 0.104 S = 1.06 4435 reflections 306 parameters 6 restraints Hydrogen site location: mixed H atoms treated by a mixture of independent and constrained refinement w = 1/[σ2(Fo2) + (0.0467P)2 + 0.8165P] where P = (Fo2 + 2Fc2)/3 (Δ/σ)max = 0.002 Δρmax = 0.89 e Å−3 Δρmin = −0.66 e Å−3 supporting information sup-8Acta Cryst. (2023).



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